fig6

Figure 6. XRD patterns of LOTC sample 8: (a) before DSC heating, (b) after DSC heating to 210 oC, (c) after DSC heating to 250 oC, and (d) after DSC heating to 300 oC. LOTC: 1.6Li2O-TaCl5; XRD: X-ray diffraction; DSC: differential scanning calorimetry.