fig4

Lithium-rich, oxygen-deficient spinel obtained through low-temperature decomposition of heterometallic molecular precursor

Figure 4. Powder X-ray diffraction pattern of the decomposition residue of precursor 1 at 310 oC and the Le Bail fit for the cubic unit cell (Sp. gr. Fd-3m) with a = 8.1170(1) Å. The black and blue curves are the experimental and calculated patterns, respectively. The grey line is the difference curve. Theoretical peak positions are shown as blue bars at the bottom.

Energy Materials
ISSN 2770-5900 (Online)
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