fig4
Figure 4. (A) UV-vis absorption spectra of the supernatant of Li2S6 solution with 3D Ti3C2Tx and 3D N-Ti3C2Tx and the inset is a digital photograph. XPS pattern: (B) N 1s and (C) S 2p of 3D N-Ti3C2Tx after adsorption of Li2S6. The CV curves of symmetric cells with electrolytes containing Li2S6, (D) scan rate: 0.2 mV s-1 and (E) scan rate: 10 to 50 mV s-1 (3D N-Ti3C2Tx). (F) The potentiostatic discharging profiles of Li2S precipitation (at 2.05 V) for 3D N-Ti3C2Tx. (G) The potentiostatic discharging profiles of Li2S dissolution (at 2.35 V) for 3D N-Ti3C2Txand 3D Ti3C2Tx. (H) Tafel plot. (I) The EIS plot of 3D N-Ti3C2Tx symmetrical battery containing Li2S6 electrolytes at different temperatures.